Home Microbiology A Rapid, Scalable Method for the Isolation, Functional Study, and Analysis of Cell-derived Extracellular Matrix
Microbiology JoVE (Open Access) Citable · DOI

A Rapid, Scalable Method for the Isolation, Functional Study, and Analysis of Cell-derived Extracellular Matrix

DOI: 10.3791/55051-v
What you'll learn
  • Isolate cell-derived extracellular matrix using ammonium hydroxide decellularization
  • Prepare sterile ECM for functional cell assays and downstream applications
  • Analyze ECM composition via SDS-PAGE, immunoblotting, and proteomics
Protocol

The extracellular matrix plays a major role in defining the microenvironment of cells and in modulating cell behavior and phenotype. We describe a rapid method for the isolation of cell-derived extracellular matrix, which can be adapted to different scales for microscopic, biochemical, proteomic, or functional studies.

Difficulty
intermediate
Total time
~2–4 hours per sample (depending on scale and downstream analysis)
Model organism
Cell culture (fibroblasts and other cell types)
Biosafety
BSL-1

Steps

1
Remove cells with ammonium hydroxide solution

Treat cell-seeded surfaces with ammonium hydroxide to selectively lyse and remove cellular material while preserving the underlying extracellular matrix.

▶ 00:56
2
Prepare sterile ECM for functional assays

Process decellularized matrix under sterile conditions and prepare it for use in cell functional studies and behavior assays.

▶ 03:21
3
Isolate ECM for biochemical and proteomic analysis

Collect and process the isolated extracellular matrix for protein extraction, SDS-PAGE, immunoblotting, and mass spectrometry-based proteomics.

▶ 05:01
4
Analyze isolated ECM composition and structure

Characterize the recovered extracellular matrix using microscopy, biochemical assays, and molecular profiling to confirm successful isolation and assess matrix properties.

▶ 06:30
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