Home Biochemistry Detection of Post-translational Modifications on Native Intact Nucleosomes by ELISA
Biochemistry JoVE (Open Access) Citable · DOI

Detection of Post-translational Modifications on Native Intact Nucleosomes by ELISA

DOI: 10.3791/2593-v
What you'll learn
  • Isolate native intact nucleosomes from cell nuclei using micrococcal nuclease digestion
  • Quantify histone post-translational modifications (methylation, acetylation, phosphorylation) via NU-ELISA
  • Assess global chromatin modification patterns in specific cell types
Protocol

Nucleosome ELISA (NU-ELISA) is a sensitive and quantitative method to detect global patterns of post-translational modifications in preparations of native, intact nucleosomes. These modifications include methylations, acetylations, and phosphorylations at specific histone amino acid residues, and hence NU-ELISA provides a global proteomic assay of the overall chromatin modification states of specific cell types.

Difficulty
advanced
Total time
~4–6 hours per sample preparation and ELISA assay
Biosafety
BSL-1

Steps

1
Isolate cell nuclei from tissue or culture

Extract nuclei from cells using standard nuclear isolation protocols. This step prepares intact nuclei for subsequent chromatin digestion.

▶ 01:26
2
Digest chromatin with micrococcal nuclease in situ

Treat isolated nuclei with micrococcal nuclease to selectively cleave linker DNA and release native, intact nucleosomes. Optimize digestion to preserve nucleosome structure.

▶ 03:07
3
Perform nucleosome-ELISA to detect modifications

Capture nucleosomes on ELISA plates and detect specific histone post-translational modifications using modification-specific antibodies. Quantify signal to determine global modification patterns.

▶ 04:31
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