Failure Case Library

Real lab failures, root causes, and fixes — curated and bilingually annotated by our team.

All Techniques (18) PCR (Sigma Guide) (12) End-point PCR Primers (9) Western Blot (9) Wound Healing Assay (5) Cell Culture (Contamination) (7) Lipid Transfection (8) CCK-8 Cell Viability Assay (5) Colony Formation Assay (10) Transfection (8) Nucleic Acid Quantification (9) Transfection (Co-transfection) (1) Protein Extraction (4) Plasmid Construction (Double Digest) (1) Sanger Sequencing (2) Plasmid Construction (1) qPCR (RT-qPCR) (5) Transwell Migration / Invasion Assay (5) Immunohistochemistry (IHC) (6) PCR (Polymerase Chain Reaction) (26) Restriction Enzyme Digest (13) DNA Cleanup & Plasmid Purification (7) RNA Cleanup (4) NGS Library Preparation (NEBNext Ultra II) (7) HMW DNA Extraction (Monarch) (7) LAMP (Loop-mediated Isothermal Amplification) (7) RNA Depletion for RNA-seq (7) Bacterial rRNA Depletion (4) Cell-free DNA Extraction (8) ELISA (Competitive) (18) ELISA (Signal Problems) (11) ELISA (High Background) (8) ELISA (Inconsistent Results / High CV) (6) ELISA (Standard Curve Fit Problems) (6) Western Blot (Weak / No Signal) (6) Western Blot (Detection Problems) (7) Western Blot (Bands at Wrong MW) (5) Western Blot (Misshapen / Uneven Bands) (5) Western Blot (Unexpected Multiple Bands) (7) Western Blot (Unusual Gel Band Appearance) (3) ChIP (High Background) (1) ChIP (Low Resolution with High Background) (6) ChIP (Low Signal) (8) ChIP (PCR Amplification Problems) (4) Immunohistochemistry (High Background) (9) Immunohistochemistry (No Staining) (9) Immunoprecipitation (High Antibody Elution) (1) Immunoprecipitation (High Background) (8) Immunoprecipitation (No Protein Detected) (5) Immunoprecipitation (Protein Obstruction) (1) ELISPOT (8) Tissue Imaging (Autofluorescence) (9) Flow Cytometry (Troubleshooting) (8) ELISA Development (9) Flow Cytometry (Autofluorescence) (7) Flow Cytometry (Compensation) (7) Flow Cytometry (Fc Blocking) (7) Flow Cytometry (Fixation & Permeabilization) (9) Flow Cytometry (Isotype Controls) (7) Flow Cytometry (Fixation Buffers) (7) Western Blot (CST Guide) (8) ChIP (CST Guide) (8) Immunoprecipitation (CST Guide) (14) Immunohistochemistry (CST Guide) (14) Flow Cytometry (CST Guide) (8) ELISA (R&D Guide) (10) ELISA (Sigma Guide) (6) Western Blot Immunodetection (19) IP-Western Blot (6) Flow Cytometry (Sample Considerations) (14) Flow Cytometry (Paraformaldehyde Fixation) (14) Western Blot (Sigma Protocol) (8) PCR / RT-PCR Amplification Problems (5) Cell Culture (Cell Death) (8) Cell Culture (Precipitates) (6) PCR (Invitrogen Guide) (8) PCR / qPCR Plastics (9) Flow Cytometry (Controls) (8) Plasmid Mini-prep (1) Transfection (siRNA Knockdown) (1) Western Blot (Blue Background) (1)
ELISA (Competitive) moderate

High CVs at Bottom of Standard Curve

Coefficient of variation (CV) among replicates is excessively high at the lowest standard concentrations (highest OD in competitive format), reducing precision at the sensitive end of the curve.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

Standard Curve Plateau at High Concentration End

The standard curve reaches a plateau at high analyte concentrations (low OD values in competitive format), showing no further decrease in signal despite increasing standard concentration.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

OD Value of Zero Standard Too Low

The zero standard (maximum binding, no competitor) shows insufficient optical density signal, providing inadequate dynamic range for the competitive assay and poor B/B0 calculations.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) critical

No Signal for Standard Curve with Normal Zero Standard

All standard concentrations show no signal (high OD in competitive format similar to zero standard), while the zero standard (no competitor) shows normal maximum binding signal.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) moderate

B/B0 Ratio at Standard Curve Endpoint Out of Range

The B/B0 ratio (bound/maximum bound) at the lowest or highest standard concentration is either >95% or <5%, indicating the standard curve dynamic range is not properly positioned.

💡 3 causes ✓ 3 fixes
ELISA (Competitive) severe

Non-specific Background Signal Too High in Competitive ELISA

High background optical density is observed across wells, reducing signal-to-noise ratio and making it difficult to distinguish specific binding from non-specific interactions.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

Standard Curve Plateau at High Concentration Range

The standard curve reaches a plateau (flat response) at high standard concentrations with correspondingly low OD values, failing to show expected dose-response relationship in competitive ELISA format.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) critical

Absent Standard Curve Signal with Normal Zero Standard

No detectable signal is observed for standard curve points containing analyte, while the zero standard (maximum binding control) shows normal OD values, indicating complete loss of competitive inhibition.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) moderate

High Coefficient of Variation at Lower Standard Curve

Replicate measurements at the bottom of the standard curve (highest OD values, lowest analyte concentrations) show excessive variability with high coefficient of variation (CV) between replicates.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

Low OD Value for Zero Standard in Competitive ELISA

The zero standard (B0, representing maximum antibody binding without competing analyte) produces lower than expected optical density values, reducing overall assay sensitivity and dynamic range.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

B/B0 Ratio at Curve Endpoint Outside 5-95% Range

The B/B0 ratio (bound/maximum bound signal) for the highest or lowest standard concentration exceeds 95% or falls below 5%, indicating the standard curve dynamic range does not adequately cover the analyte concentration range.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

High Non-Specific Background Signal in Competitive ELISA

Elevated background signal is detected across wells, interfering with specific signal measurement. Background noise reduces assay sensitivity and may mask low-concentration analyte detection.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) critical

Complete Absence of Standard Curve Signal with Normal Zero

All standard concentrations show no detectable signal (very low OD), while the zero standard (B0, maximum binding) produces normal expected signal, indicating complete competition failure.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

B/B0 Ratio Outside Acceptable Range at Curve Endpoints

The B/B0 ratio (bound/maximum bound) for the terminal point of the standard curve is either >95% or <5%, indicating insufficient competitive displacement range.

💡 3 causes ✓ 3 fixes
ELISA (Competitive) moderate

Standard Curve Plateau at High Concentration End

The top of the standard curve (high analyte concentration, low OD) shows a plateau with minimal signal change across multiple high-concentration standards, reducing dynamic range.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

Insufficient Signal from Zero Standard (B0)

The zero standard (no competing antigen, maximum antibody binding) produces OD values that are too low, resulting in compressed standard curve with poor sensitivity.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) moderate

High Coefficient of Variation at Low Standard Concentrations

Replicate wells at the bottom of the standard curve (low analyte, high OD) show high CVs >15-20%, while mid-curve and high-concentration points demonstrate acceptable reproducibility.

💡 4 causes ✓ 4 fixes
ELISA (Competitive) severe

Excessive Non-Specific Background Signal in Competitive ELISA

High background optical density readings are observed across wells, obscuring the difference between standards and samples. Signal persists even in wells without primary antibody or sample.

💡 4 causes ✓ 4 fixes